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  • Chloralkali process

    11 June 2011 ( #Experiments )

    Warning: Chloralkali process can release toxic chlorine vapor and sodium hydroxide, which is corrosive. Research conditions before attempting electrolysis on a substance. Only release halogens outside, in a fume hood, or in a test tube. The chloralkali...

  • How to Obtain Elements--Lithium

    09 June 2011 ( #Elements )

    As I had stated in an earlier post, I have compiled a list of sources for the elements that are available to the amateur chemist. Lithium will be discussed here. Lithium is a soft, malleable, gray alkali metal. It tarnishes to purple, then black, then...

  • How to Obtain Elements--Fluorine

    16 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Fluorine will be discussed here. Fluorine is the most reactive element. It is an extremely powerful oxidizing agent. It is a yellow-brown toxic gas. Fluorides,...

  • How to Obtain Elements--Carbon

    13 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Carbon will be discussed here. Carbon has several physical forms, or allotropes. Graphite is black, soft, electrically conductive solid. Diamond is a clear,...

  • Gallium Alloys

    26 February 2012 ( #Experiments )

    Recently I produced zinc- and aluminium-gallium alloys. There are two ways to do this with zinc. The first method is to react zinc with an acidic solution of a gallium salt. The gallium produced dissolves in the zinc metal to form the alloy containing...

  • High Temperature Oxidation of Elements

    17 June 2011 ( #Experiments )

    Warning: Many metal oxide fumes and other oxides are harmful for inhalation. Do not burn yourself on the hot materials. Arsenic, selenium, lead, and tellurium are quite toxic. You will need: One or more of these: lead powder, bismuth powder, tellurium...

  • How to Obtain Elements--Sodium

    20 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Sodium will be discussed here. Sodium is a light, low-melting, reactive metal. It belongs in the alkali metals group. It oxidizes rapidly in air, and its reaction...

  • Beryllium Dissolution

    26 February 2012 ( #Experiments )

    I tried dissolving my beryllium lump. Placement in 5% acetic acid resulted in no reaction. In this regard beryllium (and its protective layer) are very similar to aluminium. Placement in concentrated hydrochloric acid, however, resulted in a vigorous...

  • Periodate Production

    28 February 2012 ( #Experiments )

    The production of sodium periodate is very simple. You need tincture of iodine and sodium hypochlorite. Add the sodium hypochlorite to the tincture of iodine. The triiodide ion is oxidized to hypoiodite, whichly quickly oxidizes to iodate, then gradually...

  • How to Obtain Elements--Chlorine

    27 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Chlorine will be discussed here. Chlorine is a light yellow-green gas. It is the second halogen. It is less oxidizing than fluorine but more oxidizing than bromine....

  • How to Obtain Elements--Magnesium

    21 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Magnesium will be discussed here. Magnesium is a light, relatively strong alkali metal. It is highly reactive but protected by an oxide layer. It finds much...

  • How to Make Cobalt Oxides

    05 July 2011 ( #Experiments )

    Warning: Cobalt compounds are toxic and potentially carcinogenic. Do not ingest or inhale them. Bleach fumes may be a problem. The procedures that release chlorine should be done under a fume hood or outdoors. You will need: Test tube Cobalt(II) chloride...

  • How to Obtain Elements--Sulfur

    25 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Sulfur will be discussed here. Sulfur is a yellow crystalline substance. It is a brittle flammable nonmetal. It burns to make the noxious gas sulfur dioxide....

  • How to Obtain Elements--Calcium

    30 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Calcium will be discussed here. Calcium is a somewhat soft, silvery-gray metal. It reacts with water to produce white calcium hydroxide and hydrogen gas. Calcium...

  • Copper(II) ammine complex

    14 June 2011 ( #Experiments )

    Warning: Copper salts are toxic. Do not eat or drink. We have already seen the copper(I) ammine complex, which is colorless. It was formed when copper(I) oxide dissolves in ammonia. When it was oxidized, a blue solution of the copper(II) ammine complex...

  • How to Obtain Elements--Iron

    07 July 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Iron will be discussed here. Iron is the most common structural metal in the world. It is very strong, cheap, and sturdy. It is the second most common metal...

  • Comproportionation Reaction

    02 March 2012 ( #Experiments )

    A comproportionation reaction sounds extremely complicated. In reality it is quite simple.Two differently charged atoms orr ions of the same element react to form two equally charged ions. Three common examples will be discussed. First: Copper. When an...

  • Copper(II) Chloride - Dissolution of Metals

    05 March 2012 ( #Experiments )

    Copper(II) chloride has a unique ability to partially remove the protective oxide layers from aluminium. Copper sulfate, a more common copper compound, does not behave this way with aluminium. Why does copper(II) chloride have this ability? Does copper(II)...

  • How to Obtain Elements -- Zinc

    12 March 2012 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Zinc will be discussed here. Zinc is a relatively soft, bluish colored metal from Group 12. It is sometimes considered a transition metal and sometimes a post-transition...

  • Copper(II) chloro complexes

    13 June 2011 ( #Experiments )

    Warning: Copper compounds are toxic. Do not eat or drink. Hydrochloric acid is corrosive. Wear gloves. You will need: Copper(II) chloride Hydrochloric acid Test tube Copper(II) chloride forms chloro complexes with hydrochloric acid. They range in color...

  • How to Obtain Elements--Neon

    17 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Neon will be discussed here. Neon is another noble gas. It is colorless, odorless, and tasteless. It forms no known compounds. It is used in neon lamps. It is...

  • The Dissolving of Lead

    07 March 2012 ( #Experiments )

    Lead is a unique metal to dissolve as its chloride and sulfate are relatively insoluble. Therefore, hydrochloric and sulfuric acids are not the ideal choice for dissolving lead. Sulfuric acid: Sulfuric acid dissolution of lead does not work without an...

  • Silver Compounds in Light

    06 March 2012 ( #Experiments )

    Silver halides are light sensitive, making them useful for old-time film photography. Silver chloride, a white solid, has the quickest reaction with light. It turns purplish after about one minute in strong sunlight. Upon further exposure, it turns black,...

  • How to Obtain Elements--Aluminium

    22 June 2011 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Aluminium will be discussed here. Aluminium is a very common, light, silvery gray metal. It requires much energy to extract from its ores and can be recycled...

  • How to Obtain Elements -- Gallium

    13 March 2012 ( #Elements )

    I have compiled a list of sources for the elements that are available to the amateur chemist. Gallium will be discussed here. Gallium is a soft, low-melting metal. It can even melt in the human hand. Gallium is found beneath aluminium on the periodic...

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